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HRID469813

反应详情

EQUATION

反应方程式

HRID 469813 的结构方程式

REACTANTS

反应物

1
结构：CC1(C)OB(c2ccc(N)c([N+](=O)[O-])c2)OC1(C)C
HCID16217914

2-Nitro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

C12H17BN2O4

PRODUCTS

生成物

1
结构：CC1(C)OB(c2ccc(N)c(N)c2)OC1(C)C
HCID17750242

4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)benzene-1,2-diamine

C12H19BN2O2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Ni]
催化剂HCID935

Nickel

Ni

PROCEDURE

实验过程

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzene-1,2-diamine is prepared from the commercially available 2-nitro-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenylamine using the Ra—Ni catalyzed nitro reduction method described in Example 1 (step c).