HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 1-Bromo-5-(tert-butyl)-4-methoxy-2-nitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | 2-Tert-butyl-4-bromo-5-nitrophenol | HCID 57470236 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 1-Bromo-5-(tert-butyl)-4-methoxy-2-nitrobenzene | HCID 57470245 | 69.4% |
Reaction Steps
To a mixture of 2-tert-butyl-4-bromo-5-nitrophenol (C-14-a) (1.5 g, 5.5 mmol) and Cs2CO3 (2.2 g, 6.6 mmol) in DMF (6 mL) was added methyl iodide (5150 μL, 8.3 mmol). The mixture was stirred at room temperature for 4 h, diluted with H2O and extracted twice with EtOAc. The combined organic layers were washed with brine and dried over MgSO4. After removal of solvent, the residue was washed with hexane to yield 1-tert-butyl-2-methoxy-5-bromo-4-nitrobenzene (1.1 g, 69%). 1H NMR (400 MHz, CDCl3) δ 7.58 (s, 1H), 7.44 (s, 1H), 3.92 (s, 3H), 1.39 (s, 9H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629162B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-cf60ac4f10c14fc8b1167a86e506a299 |
| Source note | uspto-grants-2014_01 |