HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dichloro-4,6-dinitrobenzene → 4,6-Dichlorobenzene-1,3-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dichloro-4,6-dinitrobenzene | HCID 77286 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 4,6-Dichlorobenzene-1,3-diamine | HCID 3372869 | — |
Reaction Steps
4,6-Dichloro-benzene-1,3-diamine (D-2) was synthesized following the general scheme above starting from 1,5-dichloro-2,4-dinitro-benzene. Yield (95%). HPLC ret. time 1.88 min, 10-99% CH3CN, 5 min run; ESI-MS 177.1 m/z (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629162B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-b26f3590dedb4e62ba3bca723084e02a |
| Source note | uspto-grants-2014_01 |