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HRID470062

反应详情

EQUATION

反应方程式

HRID 470062 的结构方程式

REACTANTS

反应物

1
结构：COc1ccc([N+](=O)[O-])cc1[N+](=O)[O-]
HCID8385

2,4-Dinitroanisole

C7H6N2O5

PRODUCTS

生成物

1
结构：COc1ccc(N)cc1N
HCID11976

2,4-Diaminoanisole

C7H10N2O

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

4-Methoxy-benzene-1,3-diamine (D-3) was synthesized following the general scheme above starting from 1-methoxy-2,4-dinitro-benzene. Yield (quant.). HPLC ret. time 0.31 min, 10-99% CH3CN, 5 min run.

WORKUP

后处理

  1. customYield (quant.)