huagongshe.com
HRID470446

反应详情

EQUATION

反应方程式

HRID 470446 的结构方程式

REACTANTS

反应物

2
结构：Cn1ccc(I)cc1=O
HCID53408009

4-Iodo-1-methylpyridin-2(1H)-one

C6H6INO

结构：C[C@@H](c1ccc(B2OC(C)(C)C(C)(C)O2)cc1)N1CC[C@](CC(C)(C)O)(c2ccccc2F)OC1=O
HCID59635798

未命名化合物

PRODUCTS

生成物

1
结构：C[C@@H](c1ccc(-c2ccn(C)c(=O)c2)cc1)N1CC[C@](CC(C)(C)O)(c2ccccc2F)OC1=O
HCID59635741

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from (S)-6-(2-fluorophenyl)-6-(2-hydroxy-2-methyl propyl)-3-((S)-1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethyl)-1,3-oxazinan-2-one and 4-iodo-1-methylpyridin-2(1H)-one following a procedure analogous to that described in Example 23 Step 9. LC-MS Method 2 tR=1.58 min, m/z=501, 479, 421.