HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Iodo-1-methylpyridin-2(1H)-one → HCID 59635717, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Iodo-1-methylpyridin-2(1H)-one | HCID 53408009 | — |
| Reactant | HCID 66736273 | HCID 66736273 | — |
| Product | HCID 59635717 | HCID 59635717 | — |
Reaction Steps
The title compound was prepared from (S)-6-(3-fluorophenyl)-6-(2-hydroxy-2-methylpropyl)-3-((S)-1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethyl)-1,3-oxazinan-2-one and 4-iodo-1-methylpyridin-2(1H)-one following a procedure analogous to that described in Example 23 Step 9. LC-MS Method 2 tR=1.57 min, m/z=501, 479, 421.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629138B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-ca9027e3e336483f9fda25b00b0ee986 |
| Source note | uspto-grants-2014_01 |