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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 470573Generated: October 29, 2026

HCID 58102395, compound → HCID 49800385, compound

https://huagongshe.com/reaction/470573

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 58102395HCID 58102395—
Reactant4-Bromo-1-cyclopropylpyridin-2(1H)-oneHCID 59635647—
ProductHCID 49800385HCID 49800385—

Reaction Steps

The title compound was prepared from (S)-6-(2-hydroxy-2-methyl-propyl)-3-{(S)-1-[3-methyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-6-phenyl-[1,3]oxazinan-2-one and 4-bromo-1-cyclopropyl-1H-pyridin-2-one following a procedure analogous to that described in Step 5 of Example 96. LC-MS (Method 5): tR=3.42 min; Mass spectrum (ESI+): m/z=501 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08629138B2
Source datasetuspto-grants-2014_01
ORD IDord-47ddcadf978e4fbe85eea752e391e3a0
Source noteuspto-grants-2014_01