HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58102395, compound → HCID 49800385, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58102395 | HCID 58102395 | — |
| Reactant | 4-Bromo-1-cyclopropylpyridin-2(1H)-one | HCID 59635647 | — |
| Product | HCID 49800385 | HCID 49800385 | — |
Reaction Steps
The title compound was prepared from (S)-6-(2-hydroxy-2-methyl-propyl)-3-{(S)-1-[3-methyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-6-phenyl-[1,3]oxazinan-2-one and 4-bromo-1-cyclopropyl-1H-pyridin-2-one following a procedure analogous to that described in Step 5 of Example 96. LC-MS (Method 5): tR=3.42 min; Mass spectrum (ESI+): m/z=501 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629138B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-47ddcadf978e4fbe85eea752e391e3a0 |
| Source note | uspto-grants-2014_01 |