HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropanecarbonyl chloride → 4,4-Dimethyl-7-(cyclopropylcarbonyl-amino)-8-nitro-2H,4H-isoquinoline-1,3-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropanecarbonyl chloride | HCID 77637 | — |
| Reactant | 4,4-dimethyl-7-acetamino-8-nitro-2H,4H-isoquinoline-1,3-dione | HCID 11833171 | — |
| Product | 4,4-Dimethyl-7-(cyclopropylcarbonyl-amino)-8-nitro-2H,4H-isoquinoline-1,3-dione | HCID 20384929 | — |
Reaction Steps
Prepared analogous to Example 1b from 5.8 gm of 4,4-dimethyl-7-acetamino-8-nitro-2H,4H-isoquinoline-1,3-dione and 6.3 gm of cyclopropane carboxylic acid chloride (heating time: 30 hours).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04176184 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-4f6df2d7ae0e44b3a1857c035bfd45ad |
| Source note | uspto-grants-1979_11 |