HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Dimethylamino)propyl chloride hydrochloride → 7,7-Dimethyl-2-phenyl-5-(3-dimethylamino-propyl)-5H,7H-imidazo[4,5-h]isoquinoline-4,6-dione dihydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Dimethylamino)propyl chloride hydrochloride | HCID 94308 | — |
| Reactant | 7,7-Dimethyl-2-phenyl-5H,7H-imidazo[4,5-h]isoquinoline-4,6-dione hydrochloride | HCID 70610449 | — |
| Product | 7,7-Dimethyl-2-phenyl-5-(3-dimethylamino-propyl)-5H,7H-imidazo[4,5-h]isoquinoline-4,6-dione dihydrochloride | HCID 70610295 | — |
Reaction Steps
Prepared analogous to Example 23 from 3.4 gm of 7,7-dimethyl-2-phenyl-5H,7H-imidazo(4,5-h]isoquinoline-4,6-dione hydrochloride and 1.7gm of 3-dimethylamino-propyl chloride hydrochloride (reaction temperature: 50°-60° C.; reaction time: 18 hous).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04176184 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-861f45d8930049aebc72cc5caecb3e47 |
| Source note | uspto-grants-1979_11 |