HuagongsheHuagongshe Chemistry Print Report · For research reference only
cis-1-hydroxy-3-(1,1-dimethylheptyl)-6,6-dimethyl-6,6a,7,8,10,10a-hexahydro-9H-dibenzo[b,d]-pyran-9-one → Nabilone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | cis-1-hydroxy-3-(1,1-dimethylheptyl)-6,6-dimethyl-6,6a,7,8,10,10a-hexahydro-9H-dibenzo[b,d]-pyran-9-one | HCID 86735145 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | Nabilone | HCID 5284592 | — |
Reaction Steps
Evaporation of the solvent from eluates shown by thin layer chromatography to contain a different component afforded 55 mg. of (-)-cis-1-hydroxy-3-(1,1-dimethylheptyl)-6,6-dimethyl-6,6a,7,8,10,10a-hexahydro-9H-dibenzo[b,d]pyran-9-one. [α]20D-50° (c=1.0, CHCl3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04176233 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-964da95d25024bbb9be94e285f40e4af |
| Source note | uspto-grants-1979_11 |