Chlorosulfamic acid → HCID 67400289, compound

HRID 471554Notes

Reaction equation

[NH2:1][C:2]1[CH:9]=[CH:8][C:7]([CH2:10][CH:11]([CH3:13])[CH3:12])=[CH:6][C:3]=1[C:4]#[N:5].[S:14](Cl)(=[O:17])(=[O:16])[NH2:15]>>[C:4]([C:3]1[CH:6]=[C:7]([CH2:10][CH:11]([CH3:13])[CH3:12])[CH:8]=[CH:9][C:2]=1[NH:1][S:14]([NH2:15])(=[O:17])=[O:16])#[N:5]

Participants

Reactant 2

HCID 24499Chlorosulfamic acid

HCID 67400670HCID 67400670, compound

Product 1

HCID 67400289HCID 67400289, compound

Procedure

Prepared as in Example 77a from 2-Amino-5-isobutylbenzonitrile (Example 88b) and sulfamoyl chloride.

Sources & evidence

ORD record: ord-7c74a3949b634be4bc582c55b612454d
Source dataset: uspto-grants-2014_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08633186B2

Reaction notes

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