HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 12916688, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Product | HCID 12916688 | HCID 12916688 | — |
Reaction Steps
Benzoyl chloride 3.0 g (0.021 mol) and 1.69 g (0.021 mol) pyridine were mixed together under nitrogen and allowed to react at room temperature overnite. Benzaldehyde 2.23 g (0.021 mol) was added and the mixture was allowed to stand at ambient temperature for 4 days. Recrystallization from ethanol:ether gave 4.27 g (0.013 mol), 62%, α-benzoyloxybenzylpyridinium chloride, mp 174.5°-176.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04727151 |
| Source dataset | uspto-grants-1988_02 |
| ORD ID | ord-538b2fa95db549c3b201e8be5d8840ea |
| Source note | uspto-grants-1988_02 |