HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxybenzyl alcohol → HCID 66746419, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxybenzyl alcohol | HCID 81437 | — |
| Reactant | Dinitrobenzonitrile | HCID 520718 | — |
| Product | HCID 66746419 | HCID 66746419 | 83% |
Reaction Steps
Prepared as in Example 111c from 2,6-dinitrobenzonitrile and 3-methoxybenzylalcohol in 83% yield. 1H NMR (400 MHz, d-DMSO) δ 3.75 (s, 3H), 5.38 (s, 2H), 6.91 (d, J=8.0 Hz, 1H), 7.04 (d, J=7.6 Hz, 1H), 7.07 (s, 1H), 7.33 (t, J=8.0 Hz, 1H), 7.78 (d, J=8.8 Hz, 4H), 7.93-7.87 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08633186B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-c7fb7ce615574edbb1fdc9349c028d47 |
| Source note | uspto-grants-2014_01 |