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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 471656Generated: October 30, 2026

3-Methoxybenzyl alcohol → HCID 66746419, compound

https://huagongshe.com/reaction/471656

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-Methoxybenzyl alcoholHCID 81437—
ReactantDinitrobenzonitrileHCID 520718—
ProductHCID 66746419HCID 6674641983%

Reaction Steps

Prepared as in Example 111c from 2,6-dinitrobenzonitrile and 3-methoxybenzylalcohol in 83% yield. 1H NMR (400 MHz, d-DMSO) δ 3.75 (s, 3H), 5.38 (s, 2H), 6.91 (d, J=8.0 Hz, 1H), 7.04 (d, J=7.6 Hz, 1H), 7.07 (s, 1H), 7.33 (t, J=8.0 Hz, 1H), 7.78 (d, J=8.8 Hz, 4H), 7.93-7.87 (m, 2H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08633186B2
Source datasetuspto-grants-2014_01
ORD IDord-c7fb7ce615574edbb1fdc9349c028d47
Source noteuspto-grants-2014_01