Dinitrobenzonitrile → HCID 66745819, compound

HRID 471693Notes

Reaction equation

HRID 471693 reaction equation
[OH:1][CH2:2][C:3]([CH3:9])([CH3:8])[C:4]([NH:6][CH3:7])=[O:5].[N+:10]([C:13]1[CH:20]=[CH:19][CH:18]=[C:17]([N+]([O-])=O)[C:14]=1[C:15]#[N:16])([O-:12])=[O:11]>>[C:15]([C:14]1[C:13]([N+:10]([O-:12])=[O:11])=[CH:20][CH:19]=[CH:18][C:17]=1[O:1][CH2:2][C:3]([CH3:9])([CH3:8])[C:4]([NH:6][CH3:7])=[O:5])#[N:16]

Participants

3

Reactant 2

HCID 520718DinitrobenzonitrileHCID 53904479HCID 53904479, compound

Product 1

HCID 66745819HCID 66745819, compoundYield 77%

Procedure

Prepared as in Example 215c from 3-hydroxy-N,2,2-trimethylpropanamide (Example 221d) and 2,6-dinitrobenzonitrile in 77% yield as a pale yellow solid. MS 378 (MH+).

Sources & evidence

ORD record
ord-f23c8d07b81049349c2e195d2cc5e439
Source dataset
uspto-grants-2014_01
Patent number
US08633186B2

Reaction notes

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