Acetyl chloride → HCID 67401087, compound

HRID 471716Notes

Reaction equation

HRID 471716 reaction equation
[CH2:1]([C:3]([CH2:19][OH:20])([CH2:17][CH3:18])[CH2:4][O:5][C:6]1[CH:13]=[CH:12][CH:11]=[C:10]([N+:14]([O-:16])=[O:15])[C:7]=1[C:8]#[N:9])[CH3:2].[C:21](Cl)(=[O:23])[CH3:22]>>[C:21]([O:20][CH2:19][C:3]([CH2:4][O:5][C:6]1[CH:13]=[CH:12][CH:11]=[C:10]([N+:14]([O-:16])=[O:15])[C:7]=1[C:8]#[N:9])([CH2:1][CH3:2])[CH2:17][CH3:18])(=[O:23])[CH3:22]

Participants

3

Reactant 2

HCID 6367Acetyl chlorideHCID 673998802-(2-Ethyl-2-(hydroxymethyl)butoxy)-6-nitrobenzonitrile

Product 1

HCID 67401087HCID 67401087, compoundYield 82%

Procedure

Prepared as in Example 231c from 2-(2-ethyl-2-(hydroxymethyl)butoxy)-6-nitrobenzonitrile (Example 232d) and acetyl chloride in 82% yield. MS 321 (MH+).

Sources & evidence

ORD record
ord-ca97659a9c9842c1b6c87e84707133f9
Source dataset
uspto-grants-2014_01
Patent number
US08633186B2

Reaction notes

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