Chlorosulfamic acid → HCID 66746175, compound

Participants

Reaction Steps

Prepared as in Example 215a from N-(4-(3-amino-2-cyanophenoxy)butyl)acetamide (Example 234b) and sulfamoyl chloride in 100% yield. 1H NMR (400 MHz, DMSO-d6) δ 1.51-1.54 (m, 2H), 1.70-1.73 (m, 2H), 1.77 (s, 3H), 3.04-3.09 (m, 2H), 4.09 (t, J=6.4 Hz, 2H), 6.93 (d, J=8.4 Hz, 1H), 7.13 (d, J=8.0 Hz, 1H), 7.25 (s, 2H), 7.54 (t, J=8.0 Hz, 1H), 7.85 (brs, 1H), 9.42 (s, 1H).

Provenance & Evidence