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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 471725Generated: November 1, 2026

Chlorosulfamic acid → HCID 86657477, compound

https://huagongshe.com/reaction/471725

Reaction equation

Participants

RoleNameHCIDCharge
ReactantChlorosulfamic acidHCID 24499—
ReactantHCID 66747022HCID 66747022—
SolventWaterHCID 962—
ProductHCID 86657477HCID 8665747763%

Reaction Steps

Prepared as in Example 215a from 2-amino-6-(4-(tert-butyldimethylsilyloxy)butoxy)benzonitrile (Example 235b) and sulfamoyl chloride in 63% yield. MS 382 (M++H2O).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08633186B2
Source datasetuspto-grants-2014_01
ORD IDord-bddd788223c94878b0fdd4bbc0f43d00
Source noteuspto-grants-2014_01