HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfamic acid → HCID 86657478, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfamic acid | HCID 24499 | — |
| Reactant | HCID 67399950 | HCID 67399950 | — |
| Product | HCID 86657478 | HCID 86657478 | 30% |
Reaction Steps
Prepared as in Example 215a from 2-amino-6-(3-hydroxypropoxy)benzonitrile (Example 238b) and sulfamoyl chloride in 30% yield. 1H NMR (400 MHz, DMSO-d6) δ 2.11-2.14 (m, 2H), 4.16-4.21 (m, 4H), 6.96 (d, J=8.0 Hz, 1H), 7.15 (d, J=7.6 Hz, 1H), 7.26 (s, 2H), 7.49 (s, 2H), 7.56 (t, J=8.4 Hz, 1H), 9.46 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08633186B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-d0afad1ae7684b57b774d1d8b1f9c3fa |
| Source note | uspto-grants-2014_01 |