HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butanethiol → HCID 67399977, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butanethiol | HCID 8012 | — |
| Reactant | Dinitrobenzonitrile | HCID 520718 | — |
| Product | HCID 67399977 | HCID 67399977 | 90% |
Reaction Steps
Prepared as in Example 215c from butane-1-thiol and 2,6-dinitrobenzonitrile in 90% yield. 1H NMR (400 MHz, CDCl3) δ 0.97 (t, J=7.2 Hz, 3H), 1.42-1.55 (m, 2H), 1.70-1.77 (m, 2H), 3.09 (t, J=7.2 Hz, 2H), 7.63-7.69 (m, 2H), 7.99-8.01 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08633186B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-9ab11733973443cdbfc8ae90d5e33e82 |
| Source note | uspto-grants-2014_01 |