Chlorosulfamic acid → HCID 67399904, compound

HRID 471737Notes

Reaction equation

[C:1]([O:4][CH:5]([CH:20]([CH3:22])[CH3:21])[C:6]([CH3:19])([CH3:18])[CH2:7][O:8][C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([NH2:15])[C:10]=1[C:16]#[N:17])(=[O:3])[CH3:2].[S:23](Cl)(=[O:26])(=[O:25])[NH2:24]>>[C:1]([O:4][CH:5]([CH:20]([CH3:22])[CH3:21])[C:6]([CH3:19])([CH3:18])[CH2:7][O:8][C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([NH:15][S:23](=[O:26])(=[O:25])[NH2:24])[C:10]=1[C:16]#[N:17])(=[O:3])[CH3:2]

Participants

Reactant 2

HCID 24499Chlorosulfamic acid

HCID 67400462HCID 67400462, compound

Product 1

HCID 67399904HCID 67399904, compoundYield 90%

Procedure

Prepared as in Example 215a from 1-(3-amino-2-cyanophenoxy)-2,2,4-trimethylpentan-3-yl acetate (Example 243b) and sulfamoyl chloride in 90% yield. MS 384 (MH+).

Sources & evidence

ORD record: ord-87c793995a524592a3a24e242a1b389a
Source dataset: uspto-grants-2014_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08633186B2

Reaction notes

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