3-Methylcyclopentan-1-ol → HCID 67400110, compound

HRID 471748Notes

Reaction equation

HRID 471748 reaction equation
[CH3:1][CH:2]1[CH2:6][CH2:5][CH:4]([OH:7])[CH2:3]1.[N+:8]([C:11]1[CH:18]=[CH:17][CH:16]=[C:15]([N+]([O-])=O)[C:12]=1[C:13]#[N:14])([O-:10])=[O:9]>>[CH3:1][CH:2]1[CH2:6][CH2:5][CH:4]([O:7][C:15]2[CH:16]=[CH:17][CH:18]=[C:11]([N+:8]([O-:10])=[O:9])[C:12]=2[C:13]#[N:14])[CH2:3]1

Participants

3

Reactant 2

HCID 867853-Methylcyclopentan-1-olHCID 520718Dinitrobenzonitrile

Product 1

HCID 67400110HCID 67400110, compoundYield 70%

Procedure

Prepared as in Example 215c from 3-methylcyclopentanol and 2,6-dinitrobenzonitrile in 70% yield. MS 247 (MH+).

Sources & evidence

ORD record
ord-e477f930453a47e399b640b31f0516a3
Source dataset
uspto-grants-2014_01
Patent number
US08633186B2

Reaction notes

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