Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(1-Methylcyclopropyl)methanol → 2-((1-Methylcyclopropyl)methoxy)-6-nitrobenzonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (1-Methylcyclopropyl)methanol | HCID 137701 | — |
| 반응물 | Dinitrobenzonitrile | HCID 520718 | — |
| 생성물 | 2-((1-Methylcyclopropyl)methoxy)-6-nitrobenzonitrile | HCID 67400354 | 65% |
반응 단계
Prepared as in Example 166d from (1-methylcyclopropyl)methanol and 2,6-dinitrobenzonitrile in 65% yield. 1H NMR (400 MHz, DMSO-d6) δ 0.44-0.46 (m, 2H), 0.57-0.59 (m, 2H), 1.22 (s, 3H), 4.06 (s, 2H), 7.67 (dd, J=1.6 Hz, J=8.0 Hz, 1H), 7.85-7.92 (m, 2H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08633186B2 |
| 출처 데이터셋 | uspto-grants-2014_01 |
| ORD ID | ord-401d151dbca942fdbe9ed711f0ebefbb |
| 출처 메모 | uspto-grants-2014_01 |