HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl Formate → Tert-butyl 3-((2-cyano-3-nitrophenoxy)methyl)piperidine-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl Formate | HCID 61207 | — |
| Reactant | Dinitrobenzonitrile | HCID 520718 | — |
| Reactant | tert-Butyl 3-(hydroxymethyl)piperidine-1-carboxylate | HCID 2763851 | — |
| Product | Tert-butyl 3-((2-cyano-3-nitrophenoxy)methyl)piperidine-1-carboxylate | HCID 66746046 | 58% |
Reaction Steps
Prepared as in Example 215c from tert-butyl 3-(hydroxymethyl)piperidine-1-carboxylate and 2,6-dinitrobenzonitrile in 58% yield. MS 263 [M+H-Boc]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08633186B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-4fb92bec1c964df2b1abbdab008f1545 |
| Source note | uspto-grants-2014_01 |