HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-cyclopentenyl-7H-pyrrolo[2,3-d]pyrimidine → 4-cyclopentyl-7H-pyrrolo[2,3-d]pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-cyclopentenyl-7H-pyrrolo[2,3-d]pyrimidine | HCID 11629712 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 4-cyclopentyl-7H-pyrrolo[2,3-d]pyrimidine | HCID 11636952 | 89% |
Reaction Steps
A mixture of 4-cyclopentenyl-7H-pyrrolo[2,3-d]pyrimidine (11 mg, 0.060 mmol) and Pd-C (10% on carbon, 22 mg) in EtOAc (1 mL) was stirred under H2 atmosphere (balloon) for 5 h. The mixture was filtered and concentrated to provide the title compound (10 mg) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08633205B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-dee465334f8f428190deeb6c62a5bd1c |
| Source note | uspto-grants-2014_01 |