HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 5-(chlorocarbonyl)-2-nitrobenzoate → HCID 67216035, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 5-(chlorocarbonyl)-2-nitrobenzoate | HCID 12350504 | — |
| Reactant | HCID 67215697 | HCID 67215697 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 67216035 | HCID 67216035 | — |
Reaction Steps
This compound is obtained according to the same process as that described in example 9 by benzoylation of tert-butyl imidazo[1,5-a]pyridine-6-carboxylate with methyl 5-(chlorocarbonyl)-2-nitrobenzoate in the presence of triethylamine. A yellow solid is obtained. Melting point: 170° C.; 1H NMR (d6-DMSO): 1.63 (9H, s), 3.89 (3H, s), 7.76 (1H, d), 8.05 (1H, s), 8.12 (1H, d), 8.26 (1H, d), 8.70 (1H, d), 8.77 (1H, s), 10.25 (1H, s)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08633216B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-6e9e4e25e72a483aba52c457cef8eabb |
| Source note | uspto-grants-2014_01 |