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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 472903Generated: October 30, 2026

Methyl 5-(chlorocarbonyl)-2-nitrobenzoate → HCID 67216035, compound

https://huagongshe.com/reaction/472903

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl 5-(chlorocarbonyl)-2-nitrobenzoateHCID 12350504—
ReactantHCID 67215697HCID 67215697—
SolventTriethylamineHCID 8471—
ProductHCID 67216035HCID 67216035—

Reaction Steps

This compound is obtained according to the same process as that described in example 9 by benzoylation of tert-butyl imidazo[1,5-a]pyridine-6-carboxylate with methyl 5-(chlorocarbonyl)-2-nitrobenzoate in the presence of triethylamine. A yellow solid is obtained. Melting point: 170° C.; 1H NMR (d6-DMSO): 1.63 (9H, s), 3.89 (3H, s), 7.76 (1H, d), 8.05 (1H, s), 8.12 (1H, d), 8.26 (1H, d), 8.70 (1H, d), 8.77 (1H, s), 10.25 (1H, s)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08633216B2
Source datasetuspto-grants-2014_01
ORD IDord-6e9e4e25e72a483aba52c457cef8eabb
Source noteuspto-grants-2014_01