HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Dioxide → Benzeneacetic acid, 4-bromo-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Dioxide | HCID 280 | — |
| Reactant | Propanedioic acid, 2-(4-bromophenyl)- | HCID 21866616 | — |
| Product | Benzeneacetic acid, 4-bromo- | HCID 74654 | 1,099.1% |
Reaction Steps
2-(4-Bromophenyl)malonic acid (36 g, 11 mmol) was heated at 165° C. until evolution of CO2. the production was crystallized from petrol ether to give 2-(4-bromophenyl)acetic acid (26 g, 87%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08633212B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-0c71970627204bb385732ec691183e7b |
| Source note | uspto-grants-2014_01 |