HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Iodobenzonitrile → HCID 60023916, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Iodobenzonitrile | HCID 144341 | — |
| Reactant | HCID 60023923 | HCID 60023923 | — |
| Product | HCID 60023916 | HCID 60023916 | 90% |
Reaction Steps
Following the procedure described for [(R)-(E)-1-isopropyl-4-(3-methoxy-phenyl)-2-oxo-but-3-enyl]-carbamic acid tert-butyl ester with 3-iodobenzonitrile (5.50 g, 24.0 mmol, 1 equiv) afforded the title compound as a yellow solid (7.4 g of ˜90% purity material). ESMS [M+H]+: 329.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08633236B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-806a24b363b34baa9e562671fb68bd62 |
| Source note | uspto-grants-2014_01 |