HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphoric Acid → HCID 54759821, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphoric Acid | HCID 1004 | — |
| Reactant | Ilorasertib | HCID 46207586 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 54759821 | HCID 54759821 | — |
Reaction Steps
N-(4-{4-amino-7-[1-(2-hydroxyethyl)-1H-pyrazol-4-yl]thieno[3,2-c]pyridin-3-yl}phenyl)-N′-(3-fluorophenyl)urea free base solid (18 mg) was suspended in 2-propanol (150 μL). Phosphoric acid solution (85%, 5 μL) was added to the suspension. The suspension was stirred at ambient temperatures for 10 days. Solid was collected by centrifuge filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08633317B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-37ddfbf1e6db4b4fba5090c11053d6d4 |
| Source note | uspto-grants-2014_01 |