Potassium Hydroxide → HCID 67359760, compound

HRID 473483Notes

Reaction equation

HRID 473483 reaction equation
C[O:2][C:3](=[O:25])[C:4]1[CH:9]=[CH:8][C:7]([N+:10]([O-:12])=[O:11])=[CH:6][C:5]=1[CH2:13][O:14][C:15]1[CH:20]=[CH:19][CH:18]=[C:17]([NH:21][C:22](=[O:24])[CH3:23])[CH:16]=1.[OH-].[K+]>CO>[C:22]([NH:21][C:17]1[CH:16]=[C:15]([CH:20]=[CH:19][CH:18]=1)[O:14][CH2:13][C:5]1[CH:6]=[C:7]([N+:10]([O-:12])=[O:11])[CH:8]=[CH:9][C:4]=1[C:3]([OH:25])=[O:2])(=[O:24])[CH3:23]

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 67498122HCID 67498122, compound

Product 1

HCID 67359760HCID 67359760, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

In accordance with general method V, 1.30 g (3.78 mmol) of (3) are dissolved in 20 ml of methanol, and 0.70 g (12.50 mmol) of KOH are added. Yield 1.20 g (96.1%); melting point: 225.0° C.; C167H14N2O6 (Mr=330.30)

Sources & evidence

ORD record
ord-b5a3ecebe70848a8a20d258335de3d28
Source dataset
uspto-grants-2014_01
Patent number
US08633312B2

Reaction notes

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