HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous chloride dihydrate → 3-(2-Aminophenylamino)-8-amino-6H-dibenzo[b,e]oxepin-11-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous chloride dihydrate | HCID 61436 | — |
| Reactant | 3-(2-Nitrophenylamino)-8-nitro-6H-dibenzo[b,e]oxepin-11-one | HCID 86664809 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-(2-Aminophenylamino)-8-amino-6H-dibenzo[b,e]oxepin-11-one | HCID 45280697 | — |
Reaction Steps
In accordance with general method Y, 2.40 g (10.66 mmol) of tin(II) chloride dihydrate are dissolved in 15 ml of ethanol, and 0.35 g (0.89 mmol) of (9) is added. Yield: 0.20 g (67.9%);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08633312B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-49a901b770754a29adbcfc1819060b9e |
| Source note | uspto-grants-2014_01 |