2-Bromo-3-methylpyridine → HCID 59374317, compound

Participants

Reaction Conditions

Reaction Steps

To a 35 ml pressure vessel was added 4-(3-bromopyridin-2-yloxy)aniline (0.7095 g, 2.68 mmol) and 2-bromo-3-methylpyridine (0.575 mL, 3.35 mmol) to stir at 160° C. for 3 hours. Upon completion, the crude product was adsorbed onto a plug of silica gel and chromatographed to provide N-(4-(3-bromopyridin-2-yloxy)phenyl)-3-methylpyridin-2-amine. MS (ESI, pos. ion) m/z: 356.0.

Provenance & Evidence