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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 473765Generated: October 30, 2026

Aluminium lithium hydride → HCID 67007104, compound

https://huagongshe.com/reaction/473765

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAluminium lithium hydrideHCID 21226445—
ReactantHCID 67007225HCID 67007225—
SolventTetrahydrofuranHCID 8028—
ProductHCID 67007104HCID 6700710498.6%

Reaction Steps

To a solution of (10aR)-2,3,10,10a-tetrahydropyrazino[1,2-a]indole-1,4-dione (200 mg, 0.99 mmol) in 5 mL THF was added LAH. The reaction mixture was refluxed for 1 h. Standard work up afforded 170 mg of pure (10aR)-1,2,3,4,10,10a-hexahydropyrazino[1,2-a]indole.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08637497B2
Source datasetuspto-grants-2014_01
ORD IDord-75f8c72cd4014e9faa00a8f88944019c
Source noteuspto-grants-2014_01