HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 67007104, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 67007225 | HCID 67007225 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67007104 | HCID 67007104 | 98.6% |
Reaction Steps
To a solution of (10aR)-2,3,10,10a-tetrahydropyrazino[1,2-a]indole-1,4-dione (200 mg, 0.99 mmol) in 5 mL THF was added LAH. The reaction mixture was refluxed for 1 h. Standard work up afforded 170 mg of pure (10aR)-1,2,3,4,10,10a-hexahydropyrazino[1,2-a]indole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08637497B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-75f8c72cd4014e9faa00a8f88944019c |
| Source note | uspto-grants-2014_01 |