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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 474432Generated: October 30, 2026

HCID 66763896, compound → HCID 66763097, compound

https://huagongshe.com/reaction/474432

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 66763896HCID 66763896—
SolventHydrogen BromideHCID 260—
ProductHCID 66763097HCID 6676309713%

Reaction Steps

In a 20 mL scintillation vial 6-Benzyloxy-4-[1-(3-chloro-phenyl)-2-dimethylamino-ethylamino]-quinazoline-8-carboxylic acid amide was taken in 5 ml of aqueous HBr solution and stirred at room temperature for 2 h. Reaction was concentrated and dissolved in methanol and the crude was purified on preparative HPLC to give the product, (7.0 mg, 13% yield). LCMS (ESI) 386 (M+H)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08637532B2
Source datasetuspto-grants-2014_01
ORD IDord-ed62dc604cdb4f8d8621a5cf02df7f69
Source noteuspto-grants-2014_01