HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl butyrate → HCID 10057613, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl butyrate | HCID 7762 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 10057613 | HCID 10057613 | — |
Reaction Steps
To a suspension of potassium tert-butoxide (3.86 g, 34.4 mmol) in THF (20 mL) under nitrogen at room temperature was added a solution of ethyl butanoate (2.275 mL, 17.22 mmol) in diethyl ether (20.0 mL). The reaction mixture was stirred at rt for 3 hrs. The mixture was quenched and concentrated to give the title compound. LCMS: rt=2.34 min, [M+H+]=143
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08637536B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-f3e12b5c38d442628b2a7c8010c41a53 |
| Source note | uspto-grants-2014_01 |