HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Pyrimidin-2-ylthio)acetic acid → HCID 22172682, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Pyrimidin-2-ylthio)acetic acid | HCID 581022 | — |
| Reactant | 4-(4-amino-2-butyl 1H-imidazo[4,5-c][1,5]naphthyridin-1-yl)butaneamine | HCID 12992616 | — |
| Product | HCID 22172682 | HCID 22172682 | — |
Reaction Steps
Using the general method of Example 105 (2-pyrimidinylthio)acetic acid (0.11 g, 64 mmol) was reacted with 4-(4-amino-2-butyl-1H-imidazo[4,5-c][1,5]naphthyridin-1-yl)butaneamine (0.2 g, 0.64 mmol) to provide N1-[4-(4-amino-2-butyl-1H-imidazo[4,5-c][1,5]naphthyridin-1-yl)butyl]-2-(2-pyrimidinylsulfanyl)acetamide as a white solid, m.p. 156-160° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06699878B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-d5b0cd411f5842c0bbdf8a073d4d17d8 |
| Source note | uspto-grants-2004_03 |