反应详情

温度

140 °C

A neat mixture of 94 (691 mg, 2.67 mmol) and 53 (210 mg, 0.89 mmol) was stirred under nitrogen at 140° C. for 18 h. The dark brown mixture was cooled to RT and was purified by preparative HPLC to afford 25 mg (7.5%) of I-17 as white solid.

1. temperatureThe dark brown mixture was cooled to RT
2. customwas purified by preparative HPLC
3. customto afford 25 mg (7.5%) of I-17 as white solid