HCID 86694751, compound → HCID 86694750, compound

Participants

Reaction Steps

A solution of 262 (100 mg, 0.28 mmol) in DCM (2 mL) and TFA (2 mL) was stirred at RT for 30 min. The solvent was removed and the residue was dissolved in EtOAc and neutralized with ammonia. The organic layers were separated, washed with brine, dried (MgSO4), filtered and concentrated in vacuo to afford 40 mg (82%) of N-methyl(4-methyl-1H-benzo[d]imidazol-5-yl)methanamine (264): MS (ESI) m/z=176.3 [M+l]+.

Provenance & Evidence