HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyacetone → 2-Propanone, 1-((methylsulfonyl)oxy)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyacetone | HCID 8299 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2-Propanone, 1-((methylsulfonyl)oxy)- | HCID 146754 | — |
Reaction Steps
Thirty-seven (37) mg of hydroxyacetone was dissolved in 2 ml of chloroform, and to which 0.078 ml of methanesulfonyl chloride was added. After stirring the reaction liquid at room temperature for 30 minutes, saturated aqueous sodium bicarbonate solution was added and extracted with chloroform. The extract was dried over anhydrous sodium sulfate and concentrated to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06699880B1 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-ae0dc196daec479296ba40aa26395f87 |
| Source note | uspto-grants-2004_03 |