HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 66756492, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86592936 | HCID 86592936 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 66756492 | HCID 66756492 | — |
Reaction Steps
Ethyl (2S)-2-((tert-butoxycarbonyl)amino)-5-oxoheptanoate and trifluoroacetic acid (3 mL) were stirred in dichloromethane (3 mL) at room temperature for 3 hours. The mixture was concentrated under reduced pressure to provide the titled compound. MS (ESI) m/z 170 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08637546B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-ee3be053ec7c41acbb137cb9a80982cc |
| Source note | uspto-grants-2014_01 |