HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66756492, compound → HCID 66756635, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66756492 | HCID 66756492 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66756635 | HCID 66756635 | — |
Reaction Steps
Ethyl (2S)-5-ethyl-3,4-dihydro-2H-pyrrole-2-carboxylate dissolved in ethanol (32 mL) was stirred with 0.30 g of 10% Pd/C and under hydrogen (60 psi) for 16 hours. The catalyst was removed by filtration, and the filtrate was concentrated under reduced pressure to provide the titled compound. MS (CI) m/z 172 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08637546B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-eeef450c92b942f2a5cc410676ae2013 |
| Source note | uspto-grants-2014_01 |