HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Pentyne → Ethyl (3-(pentyne-1-yl)phenyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Pentyne | HCID 12309 | — |
| Reactant | Ethyl 3-(bromophenyl)acetate | HCID 11470552 | — |
| Reactant | 1-Butanaminium, N,N,N-tributyl-, fluoride, hydrate | HCID 16211673 | — |
| Catalyst | HCID 178418476 | HCID 178418476 | — |
| Product | Ethyl (3-(pentyne-1-yl)phenyl)acetate | HCID 67100180 | — |
Reaction Steps
heating a mixture of ethyl [3-bromophenyl]acetate and 1-pentyne in the presence of tetrabutylammonium fluoride hydrate and PdCl2(PPh3)2 to provide ethyl [3-[pentyne-1-yl]phenyl]acetate;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08637574B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-53b4b91e002c4269bcde73d56d1c0292 |
| Source note | uspto-grants-2014_01 |