HCID 178455193, compound → HCID 178489818, compound

HRID 476210Notes

Reaction equation

HRID 476210 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:20]=[C:21]([O:31][CH3:32])[C:22]=1[O:23][Si](C(C)(C)C)(C)C)/[CH:6]=[CH:7]/[C:8]1[CH:12]=[C:11]([OH:13])[N:10]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][N:15]=2)[N:9]=1.[Si](OC(C1C=NN(C2C=CC=CN=2)C=1O)=CC1C=CC=CC=1)(C(C)(C)C)(C)C>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:20]=[C:21]([O:31][CH3:32])[C:22]=1[OH:23])[CH:6]=[CH:7][C:8]1[CH:12]=[C:11]([OH:13])[N:10]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][N:15]=2)[N:9]=1

Participants

3

Reactant 2

HCID 178455193HCID 178455193, compoundHCID 178489819HCID 178489819, compound

Product 1

HCID 178489818HCID 178489818, compoundYield 94%

Procedure

The title compound was prepared in the same manner as in Example C-11, except that 1.201 mmol of Compound 9i prepared in Example C-9 was used in place of Compound 9g.

Sources & evidence

ORD record
ord-6b00583b2f424cc290e8c12a8214dff5
Source dataset
uspto-grants-2014_01
Patent number
US08637674B2

Reaction notes

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