HCID 178489819, compound → HCID 178489825, compound

HRID 476211Notes

Reaction equation

HRID 476211 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:20]=[CH:21][C:22]=1[O:23][Si](C(C)(C)C)(C)C)/[CH:6]=[CH:7]/[C:8]1[CH:12]=[C:11]([SH:13])[N:10]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][N:15]=2)[N:9]=1.COC1C=C(C=C(OC)C=1O[Si](C(C)(C)C)(C)C)/C=C/C1C=C(O)N(C2C=CC=CN=2)N=1>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:20]=[CH:21][C:22]=1[OH:23])[CH:6]=[CH:7][C:8]1[CH:12]=[C:11]([SH:13])[N:10]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][N:15]=2)[N:9]=1

Participants

3

Reactant 2

HCID 178489819HCID 178489819, compoundHCID 178489826HCID 178489826, compound

Product 1

HCID 178489825HCID 178489825, compoundYield 96%

Procedure

The title compound was prepared in the same manner as in Example C-13, except that an equimolar amount of Compound 9j prepared in Example C-10 was used in place of Compound 9i.

Sources & evidence

ORD record
ord-86b4048df4ef48fd886ffcf796956e2e
Source dataset
uspto-grants-2014_01
Patent number
US08637674B2

Reaction notes

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