HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoylacetone → HCID 67906974, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoylacetone | HCID 7166 | — |
| Reactant | 2-Morpholinoethylamine | HCID 408285 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 67906974 | HCID 67906974 | — |
Reaction Steps
A solution of 28.7 g. (0.177 mole) of benzoylacetone and 23.2 ml. (0.177 mole) of 2-(4-morpholinyl)ethylamine in 600 ml. of toluene was heated under reflux for ten and a half hours under a Dean-Stark trap and the solution then cooled and taken to dryness to give N-[2-(4-morpholinyl)ethyl]-N-(1-methyl-3-oxo-3-phenylpropenyl)amine as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04885295 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-f0b18220450b43eebcdd7796685651a4 |
| Source note | uspto-grants-1989_12 |