HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 5-Ethoxy-1,5-dihydro-2H-pyrrol-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 87710-47-2 | HCID 353549 | — |
| Product | 5-Ethoxy-1,5-dihydro-2H-pyrrol-2-one | HCID 13328432 | — |
Reaction Steps
A mixture of 2.3 g of 1,5-dihydro-5-hydroxy-2H-pyrrol-2-one in 140 cm3 of ethanol and 100 g of Amberlite resin IR-120 (H) is taken to reflux for 30 minutes. After allowing to cool, filtering off the resin and distilling the ethanol off under reduced pressure, 2.76 g of the expected product is obtained, m.p. 50°-52° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04885307 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-b86384fcb80b44178ebb443b4e54f4b1 |
| Source note | uspto-grants-1989_12 |