Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | 87710-47-2 | HCID 353549 | — |
| Product | HCID 19838067 | HCID 19838067 | — |
Reaction Steps
A mixture of 8 g of 1,5-dihydro-5-hydroxy-2H-pyrrol-2-one in 130 cm3 of benzyl alcohol and 4 g of Amberlite IR 120 H is heated for 3 hours at 60° C. The benzyl alcohol is distilled off at 65° C. under 0.3 mbar. then is drawn off under azeotropic form first with water and then with benzene. 13.6 g of the expected product is obtained, which is unstable on distilling.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04885307 |
|---|
| Source dataset | uspto-grants-1989_12 |
|---|
| ORD ID | ord-ad2103d7329d4a8f85a37c994e45dd09 |
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| Source note | uspto-grants-1989_12 |
|---|
