HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → 2-(tetrahydro-4H-thiopyran-4-yloxy)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | 2-(tetrahydro-4H-thiopyran-4-yloxy)nitrobenzene | HCID 14819599 | — |
| Catalyst | Iron | HCID 23925 | — |
| Product | 2-(tetrahydro-4H-thiopyran-4-yloxy)aniline | HCID 14819600 | 98.3% |
Reaction Steps
Following a reaction similar to that of Example 1 (2) using 5.0 g of 2-(tetrahydro-4H-thiopyran-4-yloxy)nitrobenzene, iron powder and ammonium chloride, there was obtained 4.3 g of 2-(tetrahydro-4H-thiopyran-4-yloxy)aniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04885367 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-67691ff228964e54bcb642c0226d6257 |
| Source note | uspto-grants-1989_12 |