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HRID476796

反应详情

EQUATION

反应方程式

HRID 476796 的结构方程式

REACTANTS

反应物

3
结构：[Cl-].[Cl-].[Cl-].[Dy+3]
HCID9795389

Dysprosium(III) chloride

Cl3Dy

结构：O=C(O)CN1CCNCCN(CC(=O)O)CCN(CC(=O)O)CC1.[Bi+3]
HCID86743556

未命名化合物

结构：O=[Cr](=O)(Cl)Cl
HCID178526112

未命名化合物

PRODUCTS

生成物

1
结构：O=C(O)CN1CCNCCN(CC(=O)O)CCN(CC(=O)O)CC1
HCID107830

1,4,7-tris(carboxymethyl)-1,4,7,10-tetraazacyclododecane

C14H26N4O6

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Cl-].[Cl-].[Mn+2]
催化剂HCID10313134

Manganese dichloride

Cl2Mn

CONDITIONS

反应条件

温度
88 °C

PROCEDURE

实验过程

Four hundred fifty μl of 100mM solutions of each of chromic chloride, ferric chloride, manganese chloride and dysprosium chloride were mixed with 50 μl of 1M 1,4,7-triscarboxymethyl-1,4,7,10tetraazacyclododecane and adjusted to pH 4.5. The solutions were heated at 88° C. for 20 minutes to enhance the rate of chelation, cooled and then adjusted to pH 7.

WORKUP

后处理

  1. temperaturecooled