HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 19836535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | p-Toluenesulfonic acid 1-methylheptyl ester | HCID 3912199 | — |
| Reactant | HCID 14474361 | HCID 14474361 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19836535 | HCID 19836535 | — |
Reaction Steps
The above 3'-bromo-4'-hydroxy-4-acetylbiphenyl (200 g) was treated with 1.2 times equivalents of R 1-methylheptyl p-toluenesulfonate and potassium hydroxide in 97% ethanol (1 l) for 6 hours under reflux. The reaction mixture was worked up in a usual way to obtain crude oily 3'-bromo-4'-(1-methylheptyloxy)-4-acetylbiphenyl (163 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04886622 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-a1bd88eaf8ec4544ad9ec66057274992 |
| Source note | uspto-grants-1989_12 |