HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Methyl (o-nitrobenzylthio)-acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Nitrobenzyl chloride | HCID 11921 | — |
| Reactant | Methyl Thioglycolate | HCID 16907 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Methyl (o-nitrobenzylthio)-acetate | HCID 12136843 | — |
Reaction Steps
A mixture of o-nitrobenzylchloride (17.2 g), methyl mercaptoacetate (8.9 ml), and potassium carbonate (27.6 g) was refluxed with stirring in acetone (200 ml) for 6 hours. The reaction mixture was filtered and evaporated to leave the title compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04886797 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-e4fe669c56e54387848a86e0a0daa9eb |
| Source note | uspto-grants-1989_12 |